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Publication : An electrokinetic route to rapid synthesis of nickel hydroxide and nickel oxide nanotubes.

First Author  Li XH Year  2010
Journal  J Nanosci Nanotechnol Volume  10
Issue  8 Pages  5191-5
PubMed ID  21125869 Mgi Jnum  J:169938
Mgi Id  MGI:4943614 Doi  10.1166/jnn.2010.2216
Citation  Li XH, et al. (2010) An electrokinetic route to rapid synthesis of nickel hydroxide and nickel oxide nanotubes. J Nanosci Nanotechnol 10(8):5191-5
abstractText  An electrokinetic route was developed for the synthesis of Ni(OH)2 nanotubes in the nanochannel of anodic alumina oxide (AAO) template. The nanotubes in the template were then converted to NiO nanotubes by calcination in air at 300 degrees. Uniform ordered nanotubes were obtained after selecting proper experimental conditions, such as the ionic concentration, the reaction time and the kind of nickel salts. X-ray diffraction (XRD) analysis indicated that the as-prepared Ni(OH)2 nanotubes were crystalline. Thermogravimetric analysis (TGA) was employed to determine the correlation between temperature and weight lose of the nanotubes. The transmission electron microscope (TEM) and scanning electron microscope (SEM) were used to characterize the morphology and structure of the nanotubes.
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